Contact an Account ManagerMethod development of an extraction of polar pesticides and metabolites from rape - Improvement of solvent
Summary
Type: SPE
Application #: 304340
Catalog#: 730108 - SPE Cartridges, Chromabond, HR-P, 3ml, PP, 200mg 30/pk
Detection: The extracted samples are determinated by LC/ESI-MS/MS by a polar RP column (e.g. NUCLEODUR® C18 Pyramid) with methanol / 10 mM ammonium acetate gradient.
Conditions: Column conditioning: 3 ml methanol, then 3 x 3 ml water
Sample aspiration: The prepared sample is passed through the column (vacuum: 4-5 mm Hg).
Washing: 10 ml (5% methanol in water)
Elution:
Authors: Pantiru M E
Source: Dissertation Wissenschaftszentrum Weihenstephan f&
Details
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